Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research

doi:10.7517/j.issn.1674-0475.2016.04.329

Imaging Science and Photochemistry ›› 2016, Vol. 34 ›› Issue (4): 329-335.DOI: 10.7517/j.issn.1674-0475.2016.04.329

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Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research

LI Li¹, LU Feng¹, YANG Wu²

1. Gansu Vocational & Technical College of Nonferrous Metallurgy, Jinchang 737100, Gansu,P.R.China;
2. Key Lab of Eco-Environmental Related Polymer Materials of MOE, College of Chemistry & Chemical Engineering, Northwest Normal University, Lanzhou 730070, Gansu, P.R.China

Received:2015-12-04 Revised:2016-02-29 Online:2016-07-15 Published:2016-07-15

Abstract

Abstract:

With different rotational speed of agitator, the silver nanoparticles and silver nanorods were obtained by the reduction of sodium borohydride. Then the silver nanoparticles and nanorods were self-assembed on a glass plate modified by the silane reagent 3-aminopropyltrimethoxysilane (APTMS). The glass plate was prepared as surface-enhanced Raman scattering (SERS) active basement, with Rhodamine 6G (R6G) and Rhodamine B (RB) molecular probes for the detection of the two substrates' SERS activities. The results showed that the two substrates are ideal SERS substrates.

Key words: silver nanoparticles, silver nanorods, self-assembled, SERS

LI Li, LU Feng, YANG Wu. Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research[J]. Imaging Science and Photochemistry, 2016, 34(4): 329-335.

References

[1] 沈剑沧.银纳米颗粒的合成与表面增强拉曼光谱[J]. 兰州大学学报(自然科学版), 2007, 43(5): 139-141. Shen J C. Silver nanocrystals: synthesis and surfae-enhand Raman spectroscopy[J]. Journal of Lanzhou University, 2007,43(5): 139-141.
[2] Olson L G, LO Y S, Beebe T P, Jr and Harris J M. Characterization of silane-modified immobilized gold colloids as a substrate for surface-enhanced Raman spectroscopy[J]. Analytical Chemistry, 2001, 73(17): 4268-4276.
[3] 凌丽,徐敏敏,顾仁敖,姚建林. Ag_核Au_壳双金属复合纳米线的制备及其表面增强拉曼光谱研究[J].化学学报, 2007, 65(9): 779-784. Ling L, Xu M M, Gu R A, Yao J L. Preparation of Ag_coreAu_shell nanowires and their surface enhanced raman spectroscopic studies[J]. Acta Chimica Sinica, 2007, 65(9): 779-784.
[4] Nie S and Emory S R. Probing single molecules and single nanoparticles by surface-enhanced Raman scattering[J]. Science, 1997, 275(21): 1102-1106.
[5] 聂宜文, 张兴业, 宋延林.单分散性银纳米粒子的可控制备[J].影像科学与光化学, 2014, 32(4): 402-409. Nie Y W, Zhang X Y, Song Y L. Controllable synthesis of monodispersed silver nanoparticles[J]. Imaging Science and Photochemistry, 2014, 32(4): 402-409.
[6] Kelly K L, Coronado E, Zhao L L and Schatz G C. The optical properties of metal nanoparticles: the influence of size, shape, and dielectric environment[J]. The Journal of Physical Chemistry B, 2003, 107(3): 668-677.
[7] Sun L L, Zhao D X, Ding M, Zhao H F, Zhang Z Z, Li B H, Shen D Z. One-step synthesis of hape-controllable gold nanoparticles and their application in surface-enhanced Raman scattering[J]. Journal of Materials Science & Technology, 2013, 29(7): 613-618.
[8] Gao C Y, Chen Y C, Chen K L, Huang C J. Surface plasmon enhanced organic light emitting diodes by goldnanoparticles with different sizes[J]. Applied Surface Science, 2015, 356: 791-794.
[9] Mohammad R, Karine M, Mickael D, Ludovic J, Valeriy L, Joumana T, Kamal H, Tayssir H, Rynno L, Hamidou H. Controlling shape and spatial organization of silver crystals bysite-selective chemical growth method for improving surfaceenhanced Raman scattering activity[J]. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 2015, 484: 508-517.
[10] Westcott S L, Oldenburg S J, Lee T R and Halas N J. Formation and adsorption of clusters of gold nanoparticles onto functionalized silica nanoparticle surfaces[J]. Langmuir, 1998, 14(19): 5396-5401.
[11] Jiang Z J, Liu C Y. Seed-mediated growth technique for the preparation of a silver nanoshell on a silica sphere[J]. The Journal of Physical Chemistry B, 2003, 107(45): 12411-12415.

Preparation of Self-assembled Films of Silver Nanoparticles and Silver Nanorods for SERS Research

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[3]	DAI Jing-tao, XU Jing-kun, YANG Ping, DU Yu-kou, JIANG Long. Preparation and Characterization of Nano-Silver Particles by Conductive Polymers PEDOT/PSS Protection Method [J]. Imaging Science and Photochemistry, 2005, 23(5): 363-366.
[4]	WANG Wen-long, ZHAI Jin, BAI Feng-lian, REN Yan-jie, ZHANG Bo, CAI Sheng-min. SELF-ASSEMBLED MONOLAYER OF 3,4,9,10-PERYLENE TETRACARBOXYLIC ACID:FABRICATION,CHARACTERIZATION AND ITS PHOTOVOLTAIC BEHAVIORS [J]. Imaging Science and Photochemistry, 2002, 20(4): 262-268.
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