影像科学与光化学 ›› 1984, Vol. 2 ›› Issue (1): 1-6.DOI: 10.7517/j.issn.1674-0475.1984.01.1

• 研究论文 •    下一篇

电影胶片掉胶问题的研究

缪进康, 黄明智   

  1. 北京化工学院
  • 收稿日期:1983-01-19 出版日期:1984-02-20 发布日期:1984-02-20

A STUDY ON THE DISSOLUTION OF GELATIN FROM CINE FILM

MIAO JIN-KANO, HUANG MING-ZHI   

  1. Beijing Institute of Chemical Technology
  • Received:1983-01-19 Online:1984-02-20 Published:1984-02-20

摘要: 本文用凝胶层析法和紫外分光光度法对电影胶片掉胶问题进行了研究,得出初步结论: 1)证实了在电影胶片和加工药液中确实存在着可溶解的明胶(多肽)。 2)在室温下可从商品明胶分离得到“溶胶”和“凝胶”两个组份,“溶胶”由于复性能力较弱而易于降解。 3)提胶温度和深度是影响“溶胶”含量的重要工艺参数,先在45℃下萃取,再在50℃下提胶,可以得到“溶胶”含量很低的明胶产品,但随着提胶过程的继续进行,“溶胶”含量又将逐道增高。

Abstract: In this paper, the dissolution of gelatin from cine film into the processing solutions has been investigated by means of "gel" chromatography and UV spectrophotomethy, and the following results were obtained.1) It was proved that in the film and the processing solution there were extractable and extracted gelatins with molecular weight of 3000-30000.2) According to the solubility at room temperature, the commercial gelatins could be separated into two components "gel" (swelling component) and "sol" (soluble component). The results indicated that degradation of the "sol" goes faster than that of the "gel" due to its weaker ability of aggregation.3) The temperature and the degree of extraction are important factors effecting on the "sol" content in commercial gelatins. The product with minimum content of "sol" could be obtained by extracting gelatin at 50℃ after the extract at 45℃ had been removed. But the content of "sol" would increased with the extracting process in run by run.The experimental results showed that it is necessary to pretreat limed collagen before the extraction and control the degree of extraction, and the problem may thus be solved.