A New Method to Prepare Single-crystal Nanomaterial via

doi:10.7517/j.issn.1674-0475.2009.04.280

Abstract

Abstract: A reliable and facile new method to prepare Ni(DMG)₂ single-crystal nanomaterials was demonstrated.Single-crystal 1D nano rods and tubes with controllable size and morphology were synthesized by using classic addition reaction following with precipitation process.It provided a new method for the preparation of nanomaterials.The concentration of the reactants used as a key effective tuning parameter had been found in the work for the shape evolution.

Key words: addition reaction, nano-material, Nickel dimethylglyoxime chelate

CLC Number:

WANG Bo, ZHANG Xiu-juan, ZHANG Xiao-hong. A New Method to Prepare Single-crystal Nanomaterial via "Addition Reaction"[J]. Imaging Science and Photochemistry, 2009, 27(4): 280-286.

References

[1] Zhang J,Sun L D,Yin J L,et al.Control of ZnO morphology via a simple solution route[J].Chem.Mater.,2002,14:4172-4177.
[2] Dick K A,Deppert K,Larsson M W,et al.Synthesis of branched "nanotrees"by controlled seeding of multiple branching events[J].Nature Materials,2004,4:380-384.
[3] Trewyn B G,Whitman C M,Lin V S.Morphological control of rooln temperature ionic liquid templated mesoporous silica nanopartieles for controlled release of antibacterial agems[J].Nano Lett.,2004,4:2139-2143.
[4] 韩冬,任湘菱,陈东,等.纳米ZnO的制备及其光催化性能研究[J].感光科学与光化学(影像科学与光化学),2005,6:16-22.Han D,Ren X L,Chen D,et al.Preparation and photocatalytic property of ZnO nanopanieles[J].Photographic Science and Photochemistry(Imaging Science and Photochemistry),2005,6:16-22.
[5] Wen X G,Wang S H,Ding Y,et al.Controlled growth of large-area,uniform,vertically aligned arrays of α-Fe₂O₃nanobelts and nanowires[J].J.Phys.Chem.B,2005,109:215-220.
[6] Kang Z H,Wang E,Mao B D,et al.Controllable fabrication of carbon nanotube and nanobelt with a polyoxometalate-assisted mild hydrothermal process[J].J.Am.Chem.Soc.,2005,127:6534-6535.
[7] Kasai H,Kamatani H,Okada S,et al.Size-dependent colors and lumine-scences of organic micrcrystals[J].Jpn.J.Appl.Phys.,1996,35:L221-L223.
[8] Zhang X J,Ju W G,Zhang X H,et al.A facile route to fabrication of inorganic-small organic molecule cable-like nanocomposite arrays[J].Chem.Comm.,2005,33:4202-4204.
[9] Zhang X J,Zhang X H,Meng X M,et al.Morphology-controllable synthesis of Pyrene nanostructures and its morphology dependence of optical properties[J].J.Phys.Chem.B,2005,109:18777-18780.
[10] Li S,He L,Xiong F,et al.Enhanced fluorescent emission of organic nanoparticles of an intramoleenlar proton transfer compound and spontaneous forotation of one-dimensional nanostruetures[J].J.Phys.Chem.B,2004,108:10887-10892.
[11] Hoshino N,Inahe T,Maruyama T.Structure and optical properties of a thermochromie schiff base.thermally indueed intramolecular proton transfer in the N,N'-bis(salicylidene)-p-phenylenediamine crystals[J].Bull.Chem.Soc.Jpn.,1988,61:4207-42141.
[12] Fu H B,Yao J N.Size effects on the optical properties of organic nanoparticles[J].J.Am.Chem.Soc.,2001,123:1434-1439.
[13] Kim H Y,Bjorklund T G,Lim S H.Spectroscopic and pbotocatalytie properties of organic tetraeene nanopartieles in aqueous solution[J].Langmuir,2003,19:3941-3946.
[14] Ai S F,Lu G,Hc Q.Highly flexible pdyelectrolyte nanotubes[J].J.Am.Chem.Soc.,2003,125:11140-11141.
[15] zhng X J,Zhang X H,Lee S T.Single-crystal nanoribbons,nanotubes,and nanowires from intramolecular chargetransfer organic molecules[J].J.Am.Chem.Soc.,2007,129:3527-3532.
[16] Kasai H,Kamatani H,Yoskswa Y.Crystal size dependence of emission from perylene mieroerystals[J].Chem.Left.,1997,26:1181-1182.
[17] Debuigne F,Jeunieau L,Wiame M.Synthesis of organic nanoparticles in different W/O mieroemulsiom[J].Langmir,2000,16:7605-7611.
[18] Hu F Q,Hong Y,Yuan H.Preparation and characterization of solid lipid nanopartieles containing peptide[J].International Journal of Pharmaceutics,2004,273:29-35.
[19] Magdassi S,Moshe M.Patterning of organic nanopartieles by ink-jet printing of microemulsions[J].Langmuir,2003,19:939-942.
[20] Shikata T,Hiram H,Kotaka T.Micelle formation of detergent molecules in aqueous media.2.role of free salicyhte ions on viscoelastic properties of aqueous cetyltrimethylammonium bromide-sodium salicylate solutions[J].Langmuir,1988,4:354-359.
[21] Lianos P G,Lang J,Strazielle C,et al.Fluorescence probe study of oil-in-water microemulsions.1.effect of pentard and dodecane or toluene on some propetties of sodium dodecyl sulfate micelles[J].J.Phys.Chem.,1982,86:1019-1025.
[22] Wilkinson F,Kelly G P,Michael C.A study of the photophysical properties of various triaryl-2-pyrazotines in solution and microcrystalline form[J].J.Photochem.Photobiol.A,1990,52:309.
[23] LzMelik S,Akius D L.Superradiance of aggregated thiacarbocyanine molecules[J].J.Phys.Chem.B,1999,103:8926-8929.
[24] Fu H B,Xiao D B,Yao J N,et al.Nanofibets of 3-diphenyl-2-pyrazoline induced by cetyltrimethylammonium bromide micelles[J].Angew.Chem.Int.Ed.,2003,42:2883-2886.
[25] Hu J S,Guo Y G,Liang H P,et al.Three-dimensional self-organization of supramolecular sdf-assembled porphyrin hollow hexagonal nanoprisms[J].J.Am.Chern.Soc.,2005,127:17090-17095.
[26] Wang Z C,Medforth C J,Shelnutt J A.Porphyfin nanotubes by ionic self-assembly[J].J.Am.Chem.Soc.,2004.126:15954-15955.
[27] Liu H,Li Y,Jiang L,et al.Imaging as-grown[60] Fullerene nanotubes by template technique[J].J.Am.Chem.Soc.,2002,124:13370-13371.
[28] Kyotani T,Tsai L,Tomita A.Preparation of ultrafine carbon tubes in nanochannels of an anodic aluminum oxide film[J].Chem.Mater.,1996,8:2109-2113.
[29] Rep D B A,Roelfsema R,Esch J H van,et al.Self-assembly of low-dimensional arrays of thiophene oligomers from solution on solid substrates[J].Adv.Mater.,2000,12:563-566.
[30] Godycki L E,Rundle R E.The structure of nickel dimethylglyoxime[J].Acta.Cryst.,1953,6:487-495.
[31] Dong C J.Windows-95 based program for powder X-ray diffraction data pmcessing[J].Appl.Crystallogr.,1999,32:838.
[32] Egneus B.The solution chemistry of ethylmethylglyoxime:part II.the nickel complex[J].Anal.Chim.Acta,1969,48:291.
[33] Williams D E,Wohlauer G,Rundle R E.Crystal structures of nickel and palladium dimethylglyoximes[J].J.Am.Chem.Soc.,1959,81:755-756.
[34] Krueger G C,Miller C W A.Study in the mechanics of crystal growth from a supersaturated solution[J].J.Chem.Phys.,1953,21:2018-2023.

A New Method to Prepare Single-crystal Nanomaterial via "Addition Reaction"

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 3

Recommended Articles

Metrics

Comments

[1]	GUAN Xiaoyuan, CHEN Guangxue, HE Minghui. The Synthesis of Polyfunctional Castor Oil-based Polyurethane Acrylate by the Auxiliary of Thiol-ene Photo Click Reaction [J]. Imaging Science and Photochemistry, 2016, 34(2): 159-165.
[2]	WU Shi-kang, WANG Peng-fei. Surface Plasmon Resonance (SPR)——The Principle of a New Method for Chemical Detection [J]. Imaging Science and Photochemistry, 2008, 26(2): 157-168.
[3]	MENG JI-BEN, WEN ZHONG, WANG YONG-MEI. RESEARCH ON PHOTOADDITION REACTIONS OF THE C=N BAND---SOLID STATE PHOTO ADDITION OF BENZYLIDENEANILINE TO INDOLE [J]. Imaging Science and Photochemistry, 1994, 12(3): 248-251.