Imaging Science and Photochemistry ›› 1998, Vol. 16 ›› Issue (3): 193-196.DOI: 10.7517/j.issn.1674-0475.1998.03.193

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STUDY OF CARBON EMPTY TUBE FORMED ON DEVELOPED SILVER FILAMENTS

LIU Suwen, YUE Jun, XU Ke   

  1. Department of Applied Chemistry, University of Science & Technology of China, Hefei 230026, P. R. China
  • Received:1998-01-23 Revised:1998-04-14 Online:1998-08-20 Published:1998-08-20

Abstract: In this paper, the high resolution transmission electronic microscopy (HRTEM, resolution of 0.2 nm) is employed to observe the crystal structure of the developed silver filament from the nanometer-sized silver halide emulsions. We carry out the research work on the “empty tube” and the “core-thread” remaining in the tube after prolonged fixation. The results show that the thin string is a kind of polycrystal silver consisted of many crystalline grains, containing many microtwins and defects. There is no difference in the crystal structures between silver filaments and the core-thread. Besides, according to our observation, the empty tube is another kind carbon nanotube made up of amorphous carbon. The reaction in the empty carbon tube may become a distinctive method to prepare the various thinner nanometer-sized string.

Key words: empty tube, development, nanometer-sized silver filament