Imaging Science and Photochemistry ›› 2015, Vol. 33 ›› Issue (2): 136-143.DOI: 10.7517/j.issn.1674-0475.2015.02.136

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Effect of Hydrothermal Growing Method on the Structure and Crystalline Quality of ZnO Nanorod Array

ZHANG Meilin1,3, JIN Feng1, ZHENG Meiling1, LIU Jie1, DUAN Xuanming1,2   

  1. 1. Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, P.R.China;
    2. Chongqing Institute of Green and Intelligent Technology, Chinese Academy of Sciences, Chongqing 400714, P.R.China;
    3. University of Chinese Academy of Sciences, Beijing 100049, P.R.China
  • Received:2014-04-21 Revised:2014-05-15 Online:2015-03-15 Published:2015-03-15

Abstract:

In this work, we systematically compared the structure and crystalline quality of ZnO nanorod arrays which were prepared by three methods. According to the basic source of the hydrothermal growing solution, ZnO nanorod was prepared by using a) ammonia solution (N method), b) hexamethylene tetramine (H method) and c) alternating of 2N and H (NH method), respectively. The morphology and crystalline quality of the ZnO NW array have been characterized by using scanning electron microscopy, Raman spectroscopy, X-ray diffractometer and transmission electron microscopy. The results demonstrate that ZnO prepared with N and NH method has better orientation than that of H method, and an increasing crystalline quality trend of N

Key words: ZnO, hydrothermal method, nanorod, ZnO nanorod array